Xylem SI Analytics TitroLine 5000 Manual De Instrucciones página 79

TABLE OF CONTENT
1 Technical Specifications of the Titrator TitroLine® 5000 ................................... 81
1.1 Summary ................................................................................................................................. 81
1.2 Specifications Titrator TitroLine
1.3 Warning and safety information .............................................................................................. 84
2 Unpacking and First Operation ............................................................................ 85
2.1 Unpacking and First Operation of the titrator .......................................................................... 85
2.2 Connection and installing of Piston Burette and magnetic stirrer TM 50 ................................ 85
2.3 Connecting the Titrator - Combination with Accessories and Additional Devices .................. 86
2.3.1 Back panel of the titrator TitroLine® 5000 .............................................................................. 86
2.3.2 Connection ports of the TitroLine® 5000 . Connection of Electrodes ..................................... 86
2.3.3 Connecting a printer ................................................................................................................ 86
2.3.4 Connecting a USB device (manual controller, keyboard, memory device, hub) .................... 86
2.3.5 Connection of analytical balances ........................................................................................... 86
2.4 Setting the Language of the Country ...................................................................................... 87
2.5 Dosing unit and Accessories ................................................................................................... 89
2.6 Installing the burette tip ........................................................................................................... 90
2.7 Initial Filling and Rinsing ......................................................................................................... 91
3 Working with the Titrator TitroLine
3.1 Front Keyboard ........................................................................................................................ 93
3.2 Display ..................................................................................................................................... 93
3.3 Manual controller "mouse" ...................................................................................................... 94
3.4 External PC Keyboard ............................................................................................................. 94
3.5 Menu Structure ........................................................................................................................ 95
3.6 Main Menu ............................................................................................................................... 97
3.6.1 Automatic Titration .................................................................................................................. 97
3.6.2 Calibration (CAL menu) ........................................................................................................... 99
3.6.3 Manual Titration ..................................................................................................................... 102
3.6.4 Dosage .................................................................................................................................. 104
4 Method Parameters ............................................................................................. 106
4.1 Method editing and new method ........................................................................................... 106
4.2 Default methods .................................................................................................................... 107
4.3 Copy Methods ....................................................................................................................... 107
4.4 Delete Methods ..................................................................................................................... 108
4.5 Print method .......................................................................................................................... 108
4.6 Change Method Parameters ................................................................................................. 108
4.6.1 Method type ........................................................................................................................... 109
4.6.2 Titration mode ....................................................................................................................... 109
4.6.3 Result .................................................................................................................................... 111
4.6.4 Titration parameters .............................................................................................................. 120
4.6.5 'End-point titration' Titration parameters ............................................................................... 128
4.6.6 Dosing parameter .................................................................................................................. 129
4.6.7 Sample identification ............................................................................................................. 130
4.6.8 Documentation ...................................................................................................................... 131
5 System settings ................................................................................................... 132
5.1 Calibration settings ................................................................................................................ 132
5.2 Reagents - Dosing unit ......................................................................................................... 134
5.2.1 Replacing the dosing unit ...................................................................................................... 134
5.2.2 Replacing the titration solution .............................................................................................. 139
5.3 Globale Memory .................................................................................................................... 139
5.4 RS232 Settings ..................................................................................................................... 140
5.5 Connection of Printers ........................................................................................................... 142
5.6 Stirrer ..................................................................................................................................... 143
5.7 Date and Time ....................................................................................................................... 143
5.8 RESET .................................................................................................................................. 144
5.9 Device Information ................................................................................................................ 144
5.10 System Tone ......................................................................................................................... 145
5.11 Data exchange ...................................................................................................................... 145
5.12 Software Update .................................................................................................................... 147
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5000 .................................................................................... 82
®
5000 ........................................................... 93